2-(1,3-Dioxoisoindolin-2-yl)propanoic acid

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2-(1,3-Dioxoisoindolin-2-yl)propanoic acid

The crystal structure of the title compound, C(11)H(9)NO(4), consists of infinite one-dimensional polymeric chains due to inter-molecular O-H⋯O hydrogen bonds between the carboxyl-ate and carbonyl groups. The phthalimide ring system and the C-COO group are planar, with r.m.s. deviations of 0.0253 and 0.0067 Å, respectively, from their mean square planes and the dihedral angle between them is 66...

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2-[2-(1,3-Dioxoisoindolin-2-yl)acetamido]­acetic acid

The title mol-ecule, C(12)H(10)N(2)O(5), is non-planar with dihedral angles of 89.08 (7) and 83.21 (7)° between the phthalimide and acetamide mean planes, and the acetamide and acetic acid mean planes, respectively. In the crystal, symmetry-related mol-ecules are linked via N-H⋯O and O-H⋯O hydrogen bonds, forming an undulating two-dimensional network. There are also a number of weak C-H⋯O inter...

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(2R)-2-(1,3-Dioxoisoindolin-2-yl)-4-(methyl­sulfan­yl)butanoic acid

The title compound, C(13)H(13)NO(4)S, the 1,3-dioxoisoindolin-2-yl unit is planar (r.m.s. deviation 0.0192 Å) and is oriented at a dihedral angle of 79.14 (18)° to the carboxyl-ate group. An intra-molecular C-H⋯O hydrogen bond leads to the formation of a planar (r.m.s. deviation 0.0419 Å)R(5) ring motif. In the crystal, mol-ecules are connected through O-H⋯O and C-H⋯O hydrogen bonds with R(2) (...

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(2R)-2-(1,3-Dioxoisoindolin-2-yl)-3-methyl­butanoic acid

In the title compound, C(13)H(13)NO(4), the dihedral angle between the nine-membered phthalimino ring system and the carb-oxy-lic acid group is 67.15 (9)°. An intra-molecular C-H⋯O close contact, which forms an S(6) ring, may help to establish the mol-ecular conformation. In the crystal, mol-ecules are linked by O-H⋯O hydrogen bonds, thereby forming C(7) chains propagating in [010].

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2-(1,3-Dioxoisoindolin-2-yl)acetic acid–N′-[(E)-2-meth­oxy­benzyl­idene]pyridine-4-carbohydrazide (1/1)

In the title 1:1 cocrystal, C(10)H(7)NO(4)·C(14)H(13)N(3)O(2), mol-ecules are linked by inter-molecular C-H⋯O, N-H⋯O and O-H⋯N hydrogen bonds, forming a three-dimensional network. In addition, π-π stacking inter-actions [with centroid-centroid distances of 3.5723 (19) and 3.6158 (18) Å] are observed.

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2009

ISSN: 1600-5368

DOI: 10.1107/s1600536809040434